Number of found documents: 20917
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Influence of ball material on the resulting fatigue life of thermal sprayed HVOF coatings in dynamic impact testing
Duliškovič, J.; Daniel, Josef; Houdková, Š.
2024 - English
Dynamic impact wear, i.e. contact between two components in the presence of high cyclic local loads, is a challenging failure mode that occurs in many mechanical applications. Many previous studies have confirmed that dynamic impact testing is suitable for evaluating the contact fatigue of thermal sprayed coatings. However, the effect of the test parameters on the resulting lifetime is unclear. The aim of this study describes the effect of the ball material used in the dynamic impact test on the resulting fatigue life of the HVOF thermal sprayed coating. Three test balls made of WC/Co alloy, Si3N4 silicon nitride and 440 C steel were chosen for this study. Dynamic impaction testing was carried out on the Cr3C2-NiCr coating, which was sprayed by HVOF on a 1.2376 high-speed steel substrate. The impact lifetime was described by the number of critical impacts, i.e. the number of impacts before coating fatigue occurs. Furthermore, the depth and volume of impact craters were measured. Using scanning electron microscopy (SEM), the surface of the impacts as well as the microstructure of the coating on the cross-section in the region of the impacts were observed. Furthermore, the mechanism of crack propagation in the coating and the microstructure of the indentor were investigated. Keywords: dynamic impact test; HVOF; Cr3C2-NiCr; fatigue Available at various institutes of the ASCR
Influence of ball material on the resulting fatigue life of thermal sprayed HVOF coatings in dynamic impact testing

Dynamic impact wear, i.e. contact between two components in the presence of high cyclic local loads, is a challenging failure mode that occurs in many mechanical applications. Many previous studies ...

Duliškovič, J.; Daniel, Josef; Houdková, Š.
Ústav přístrojové techniky, 2024

Functional Tungsten-based thin films and their characterization
Košelová, Zuzana; Horáková, L.; Sobola, Dinara; Burda, Daniel; Knápek, Alexandr; Fohlerová, Z.
2024 - English
Anodizing is a technique by which thin oxide layers can be formed on a surface. Thin oxide layers have been found to be useful in a variety of applications, including emitters of electrons. Tungsten is still a common choice for cold field emitters in commercial microscopy applications. Its suitable quality can be further improved by thin film deposition. Not only the emission characteristic can be improved, but also the emitter operating time can be extended. Tungsten oxide is known for its excellent resistance to corrosion and chemical attack due to its stable crystal structure and strong chemical bonds between tungsten and oxygen atoms. Many techniques with different advantages and disadvantages have been used for this purpose. Anodization was chosen for this work because of the controllable uniform coverage of the material and its easy availability without the need for expensive complex equipment. The anodizing process involves applying an electrical potential to tungsten while it is immersed in an electrolyte solution. This creates a thin layer of tungsten oxide on the surface of the metal. The thickness and properties of the resulting oxide layer can be controlled by adjusting the anodization conditions, such as the electrolyte solution, voltage, and the duration of the process. In this work, H3PO4 was used as the electrolyte to test whether these tungsten oxide layers would be useful for electron emitters, for use in electron guns and other devices that require high-quality electron emitters. The properties were evaluated using appropriate techniques. In general, anodization of tungsten to form thin layers of tungsten oxide layers is a promising technique for producing high quality electron emitters. Keywords: cold-field emission; thin layer deposition; tungsten oxide; resonance enhanced tunneling; anodization Available at various institutes of the ASCR
Functional Tungsten-based thin films and their characterization

Anodizing is a technique by which thin oxide layers can be formed on a surface. Thin oxide layers have been found to be useful in a variety of applications, including emitters of electrons. Tungsten ...

Košelová, Zuzana; Horáková, L.; Sobola, Dinara; Burda, Daniel; Knápek, Alexandr; Fohlerová, Z.
Ústav přístrojové techniky, 2024

Microstructure modifications of Al-Si-coated press-hardened steel 22MnB5 by laser welding
Šebestová, Hana; Horník, Petr; Mika, Filip; Mikmeková, Šárka; Ambrož, Ondřej; Mrňa, Libor
2024 - English
Weld microstructure depends on the characteristics of welded materials and parameters of welding technology, especially on the heat input that determines the peak temperature and the cooling rate. When the coated sheets are welded, the effect of the chemical composition of the coating must be also considered even though its thickness is only a few tens of microns. During 22MnB5+AlSi laser welding experiments, the ferrite-stabilizing elements of coating modified the weld metal microstructure. Ferrite appeared in a quenched weld metal. The rapid cooling rate accompanying welding with a focused beam limited the homogenization of the weld metal which resulted in the formation of ferritic bands in the regions rich in Si and especially in Al. On the other hand, a high level of homogenization was reached when welding with the defocused beam. The ferritic islands uniformly distributed in the weld metal were formed at 0.4 wt% and 1.6 wt% of Si and Al, respectively. The doubled heat input reduced the Al content to 0.7 wt% insufficient for the ferrite formation at still relatively high cooling rates. Predicting the distribution of ferrite in the weld metal is challenging due to its dependence on various factors, such as cooling rate and the volume of dissolved coating, which may vary with any modifications made to the welding parameters. Keywords: laser welding; high-strength steel; microstructure; heat input; ferrite stabilization Available at various institutes of the ASCR
Microstructure modifications of Al-Si-coated press-hardened steel 22MnB5 by laser welding

Weld microstructure depends on the characteristics of welded materials and parameters of welding technology, especially on the heat input that determines the peak temperature and the cooling rate. ...

Šebestová, Hana; Horník, Petr; Mika, Filip; Mikmeková, Šárka; Ambrož, Ondřej; Mrňa, Libor
Ústav přístrojové techniky, 2024

Room temperature ethanol detection using carbon materials
Kočí, Michal
2023 - English
Allotropic forms of carbon, in particular graphene oxide (GO) or nanocrystalline diamond (NCD), attracted the attention of many research groups due to their unique electronic structures and extraordinary physical and chemical properties, preferable for many different applications, including sensor devices. This work focuses on responses of various sensing layers (NCD with hydrogen termination (H-NCD), graphene oxide (GO), reduced graphene oxide (rGO), thiol-functionalized graphene oxide (GO-SH) and their hybrid structures to ethanol vapor with concentrations up to 100 ppm in synthetic air at room temperature. The measured parameters of the tested sensors, especially stability, reproducibility and regeneration, are compared and critically evaluated. The high sensitivity of tested sensors achieved at room temperature makes them very promising for monitoring ethanol vapor as well as other volatile substances (e.g., isopropyl-alcohol or acetone). Keywords: gas sensor; nanocrystalline diamond (NCD); graphene oxide (GO); reduced graphene oxide (rGO); thiol-functionalized graphene oxide (GO-SH) Available at various institutes of the ASCR
Room temperature ethanol detection using carbon materials

Allotropic forms of carbon, in particular graphene oxide (GO) or nanocrystalline diamond (NCD), attracted the attention of many research groups due to their unique electronic structures and ...

Kočí, Michal
Fyzikální ústav, 2023

Výzkum zříceniny hradu Štamberk v kontextu regionu
Novotný, Jakub; Ramešová, Michaela
2023 - Czech
Příspěvek přibližuje dosavadní výsledky výzkumu hradu Štamberk realizovaného dle nově definovaných zásad pro výzkum, správu a prezentaci historických zřícenin, jehož cílem je podpořit nová řešení jak zvýšit využitelnost hradu pro cestovní ruch a integrovat památku do regionálních struktur lokalit s potenciálem cestovního ruchu. Hrad byl významným panstvím v rámci území dnešní Vysočiny. Předmětem řešení projektu, na kterém od roku 2020 spolupracuje ÚTAM AV ČR s Mikroregionem Telčsko, je výzkum historie hradu se zaměřením na technologická hlediska jeho výstavby, stavebních změn i zániku. Součástí je vytvoření 3D modelu zříceniny v krajinném kontextu. Projekt se soustředí na dějiny výroby vápna a související inventarizaci geologických lokalit. Tento výzkum přináší nové informace důležité nejen pro poznání historie hradu či pro studium analogických situací, ale také pro zvýšení atraktivity památky pro cestovní ruch. Příspěvek nejprve představí aktuální standardy výzkumu a managementu zřícenin, následně se bude zabývat nástinem potenciálu výzkumu Štamberka pro oblast cestovního ruchu s důrazem na historii hradu, mapování krajinného rámce a identifikace vazeb na regionální prostředí. Na závěr zrekapituluje dosavadní výsledky využitelné k prezentaci historického, kulturního i přírodního bohatství regionu se specifickou vazbou na cestovní ruch. The paper provides an overview of the research results of the Štamberk castle carried out according to newly defined principles for the research, management and presentation of historical ruins, the aim of which is to support new solutions to increase the usability of the castle for tourism and to integrate the monument into the regional structures of localities with tourism potential. The castle was an important place within the territory of today's Highlands. The subject of the project, on which ITAM CAS has been collaborating with the Telčsko Microregion since 2020, is research into the history of the castle with a focus on the technological aspects of its construction, structural changes and demise. It includes the creation of a 3D model of the ruins in a landscape context. The project focuses on the history of lime production and the related inventory of geological sites. This research brings new information important not only for learning about the history of the castle or for studying analogous situations, but also for increasing the attractiveness of the monument for tourism. The paper first presents the current standards of research and management of ruins, then it deals with an outline of the research potential of Štamberk for the field of tourism with an emphasis on the history of the castle, mapping the landscape framework and identifying links to the regional environment. At the end, it summarizes the results so far that can be used to present the historical, cultural and natural wealth of the region with a specific link to tourism. Keywords: Štamberk; ruin; technological research; presentation of monuments; tourism Available at various institutes of the ASCR
Výzkum zříceniny hradu Štamberk v kontextu regionu

Příspěvek přibližuje dosavadní výsledky výzkumu hradu Štamberk realizovaného dle nově definovaných zásad pro výzkum, správu a prezentaci historických zřícenin, jehož cílem je podpořit nová řešení jak ...

Novotný, Jakub; Ramešová, Michaela
Ústav teoretické a aplikované mechaniky, 2023

Zikmunda Hrubého z Jelení etymologický pokus
Vykypěl, Bohumil
2023 - Czech
Keywords: etymology; Zikmund Hrubý Available at various institutes of the ASCR
Zikmunda Hrubého z Jelení etymologický pokus

Vykypěl, Bohumil
Ústav pro jazyk český, 2023

Výtečník. K významové proměně jednoho pojmu
Velek, Luboš
2023 - Czech
Studie analyzuje vznik termínu „výtečník“ a jeho významové proměny v české politice a kultuře 19. a 20. století. The study analyses the emergence of the term “výtečník” and its transformations in Czech politics and culture in the 19th and 20th centuries. Keywords: political culture; Bohemia, patriotic society; Habsburg monarchy Available at various institutes of the ASCR
Výtečník. K významové proměně jednoho pojmu

Studie analyzuje vznik termínu „výtečník“ a jeho významové proměny v české politice a kultuře 19. a 20. století....

Velek, Luboš
Masarykův ústav a Archiv, 2023

Badatelské „přelety“ mezi Čechami a Moravou. Příspěvek ke vzájemné spolupráci Innocence Ladislava Červinky a Klimenta Čermáka
Velímský, Filip
2023 - Czech
Čáslavský archeolog a muzejník Kliment Čermák navázal a po dobu svého života pak i udržoval poměrně hojné styky s řadou osobností z moravské archeologické obce. Příspěvek přináší dílčí přehled těchto kontaktů s jednotlivými badateli, zejména pak Innocencem Ladislavem Červinkou, přičemž primárně vychází z dochované korespondence a rukopisů uložených v rámci Čermákovy pozůstalosti v Literárním archivu Památníku národního písemnictví v Praze, Archivu Městského muzea a knihovny v Čáslavi a Státního okresního archivu v Kutné Hoře. Do příspěvku jsou zahrnuty i zjištěné informace o vzájemném publikování textů na stránkách spolkových periodik Muzejního a vlastivědného spolku „Včela Čáslavská“, Vlasteneckého spolku muzejního v Olomouci a Moravského archeologického klubu. Kliment Čermák, the archaeologist and museum curator in Čáslav, established and during his lifetime maintained relatively abundant contacts with a number of personalities from the Moravian archaeological community. The contribution provides a partial overview of these contacts with individual researchers, especially with Innocenc Ladislav Červinka, while is primarily based on the preserved correspondence and manuscripts stored as part of Čermák's estate in the Literary Archive of the Museum of Czech Literature in Prague, the Archive of the Municipal Museum and Library in Čáslav and the State District Archive in Kutná Hora. The contribution also includes the information about the mutual publication of texts on the pages of the periodicals of the Museum and Patriotic Society „Včela Čáslavská“, the Patriotic Museum Society in Olomouc and the Moravian Archaeological Club. Keywords: Kliment Čermák; Innocenc Ladislav Červinka; archaeology; collaboration between researchers; correspondence Available at various institutes of the ASCR
Badatelské „přelety“ mezi Čechami a Moravou. Příspěvek ke vzájemné spolupráci Innocence Ladislava Červinky a Klimenta Čermáka

Čáslavský archeolog a muzejník Kliment Čermák navázal a po dobu svého života pak i udržoval poměrně hojné styky s řadou osobností z moravské archeologické obce. Příspěvek přináší dílčí přehled těchto ...

Velímský, Filip
Archeologický ústav, Praha, 2023

Ceramic protection of anti-corrosion layers of 3-glycidyloxypropyl-triethoxysilane on steel
Pokorný, P.; Prodanović, N.; Janata, Marek; Brožek, Vlastimil
2023 - English
There are various variations on the problem of steel reinforcement bond strength in concrete. Along with geometrical considerations, corrosion performance of steels with varying chemical compositions in interaction with variable chemical compositions of concrete are crucial. One approach is to cover steel surfaces with organosilane compounds, which increases the reinforcement resistance to corrosion in both acidic and alkaline conditions but, on the other hand, may weaken the reinforcement bond strength on concrete. The issue is resolved by intentionally forming a thin-walled, highly adhering corundum layer that is highly porous and impregnated with 3-glycidyloxypropyltriethoxysilane. This procedure also includes testing the adhesion properties between the ceramic and the metal and the cement prior to conducting a corrosion test in a chloride environment. Keywords: steel; concrete; ceramics Available at various institutes of the ASCR
Ceramic protection of anti-corrosion layers of 3-glycidyloxypropyl-triethoxysilane on steel

There are various variations on the problem of steel reinforcement bond strength in concrete. Along with geometrical considerations, corrosion performance of steels with varying chemical compositions ...

Pokorný, P.; Prodanović, N.; Janata, Marek; Brožek, Vlastimil
Ústav fyziky plazmatu, 2023

Application of In situ TR Spectroelectrochemical Techniques in Determination of Redox Mechanism of Bioactive Compounds
Sokolová, Romana; Jiroušková, Eliška; Degano, I.; Wantulok, J.; Nycz, J.
2023 - English
The electron transfer reactions play an important role in many natural processes. Reactions such as \ndissociation, protonation, and reactions with water and other small molecules often occur in \nbiotransformation. The reaction schemes involving these chemical reactions coupled to the \nelectron transfer can be determined by cyclic voltammetry. Additionally, in \nsitu spectroelectrochemistry can efficiently contribute to the determination of oxidation or \nreduction mechanism. This technique provides information about the electroactive chromophore during \nthe redox process allowing to identification the first reaction intermediates. The final reaction \nproducts were identified by chromatographic techniques. This study represents a key role of TR \nspectroelectrochemistry in the determination of reaction intermediates in the case of \n1,10- phenanthroline derivative substituted by bioactive phenothiazine unit and \ndrug 3- fluorophenmetrazine (2-(3-fluorophenyl)-3-methylmorpholine, 3-FPM). Co pound 3-FPM\nhave recently appeared as the new psychoactive substance in the drug market.\n Keywords: IR spectroelectrochemistry; psychoactive substances; oxidation mechanism Available on request at various institutes of the ASCR
Application of In situ TR Spectroelectrochemical Techniques in Determination of Redox Mechanism of Bioactive Compounds

The electron transfer reactions play an important role in many natural processes. Reactions such as \ndissociation, protonation, and reactions with water and other small molecules often occur in ...

Sokolová, Romana; Jiroušková, Eliška; Degano, I.; Wantulok, J.; Nycz, J.
Ústav fyzikální chemie J. Heyrovského, 2023

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