Number of found documents: 904
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Characterization of Mo-B-C nanostructured coating microstructure by means of AEM and GDOES
Buršík, Jiří; Svoboda, Milan; Švábenská, Eva; Buršíková, V.; Souček, P.; Zábranský, L.; Vašina, P.
2017 - English
A Mo-B-C nanostructured coating was prepared on WC-Co hard-metal substrate by magnetron sputtering. The details of microstructure of deposited thin layer as well as elements redistribution caused by subsequent annealing at 1000°C were studied by several experimental techniquec. Keywords: coating; nanostructure; analytical electron microscopy Available at various institutes of the ASCR
Characterization of Mo-B-C nanostructured coating microstructure by means of AEM and GDOES

A Mo-B-C nanostructured coating was prepared on WC-Co hard-metal substrate by magnetron sputtering. The details of microstructure of deposited thin layer as well as elements redistribution caused by ...

Buršík, Jiří; Svoboda, Milan; Švábenská, Eva; Buršíková, V.; Souček, P.; Zábranský, L.; Vašina, P.
Ústav fyziky materiálů, 2017

Magnetic properties of 42CrMo4 steel
Bulín, T.; Švábenská, Eva; Hapla, Miroslav; Roupcová, Pavla; Ondrušek, C.; Schneeweiss, Oldřich
2017 - English
Low alloyed high-grade chrome-molybdenum ferritic steel was investigated from the point of views of magnetic properties in dependence on heat and mechanical treatment. This steel can be used as components of magnetic circuits or some parts in electrical equipment. The basic information on structure and phase composition was obtained by optical and scanning electron microscopy, X-ray Powder Diffraction and Mössbauer Spectroscopy. The temperature stability of the material was proved by measurements of temperature dependences of magnetic moment. The magnetic parameters were obtained by measuring of magnetic hysteresis loops in dependence on saturation field and their frequencies. The results are discussed from the point of view of possible applications as a magnetic material in the very extremely environment, where high mechanical stresses and elevated temperatures can occur. Keywords: Magnetic materials; magnetic properties; steel Available at various institutes of the ASCR
Magnetic properties of 42CrMo4 steel

Low alloyed high-grade chrome-molybdenum ferritic steel was investigated from the point of views of magnetic properties in dependence on heat and mechanical treatment. This steel can be used as ...

Bulín, T.; Švábenská, Eva; Hapla, Miroslav; Roupcová, Pavla; Ondrušek, C.; Schneeweiss, Oldřich
Ústav fyziky materiálů, 2017

Fatigue crack growth in 316L under uniaxial and torsional loading
Karol, Michal; Chlupová, Alice; Mazánová, Veronika; Kruml, Tomáš
2016 - English
A study of fatigue crack initiation and growth in 316L austenitic stainless steel is reported. Fatigue experiments were performed at room temperature on full cylindrical specimens cycled axially (tension-compression) and on hollow cylindrical specimens tested in reversed torsion. Microstructure and damage evolution (crack initiation and growth) on the surface of mechanically and electrolytically polished specimens were observed using light and electron microscopy. An analysis of the orientation of microcracks and macrocracks which led to failure was made. Axially loaded specimens exhibited presence of several microcracks which resulted in macrocrack propagating perpendicularly to specimen axis. In the case of torsional loading, orientation of macrocrack propagation was dependent on applied load and presence of notches. High amount of short cracks initiated parallel to specimen axis. Long cracks exhibited a tendency to bifurcate with crack branches oriented at approximately 45° to the specimen axis. Keywords: 316L austenitic steel; surface relief; fatigue Available at various institutes of the ASCR
Fatigue crack growth in 316L under uniaxial and torsional loading

A study of fatigue crack initiation and growth in 316L austenitic stainless steel is reported. Fatigue experiments were performed at room temperature on full cylindrical specimens cycled axially ...

Karol, Michal; Chlupová, Alice; Mazánová, Veronika; Kruml, Tomáš
Ústav fyziky materiálů, 2016

NUMERICAL SUPPORT FOR STUDY OF STRESS RATIO EFFECT ON FATIGUE CRACK BEHAVIOUR IN THREE POINT BEND SPECIMEN MADE FROM VIBRATED CONCRETE
Seitl, Stanislav; Thienpont, T.
2016 - English
The fatigue behaviour of concrete has become more important for the design of structures due to more slender/slim structures, which are more sensitive to fatigue loading, or due to wind turbines, which are typically exposed to high-fatigue loading. The fatigue behaviour of concrete was investigated with respect to the influence of various stress ratios. Pilot analysis of fatigue crack propagation rate in three-point bend specimens made from ordinary vibrated concrete was done. Keywords: Stress intensity factor; fatigue crack; Paris-Erdogan law; concrete; FEM; stress ratio Available at various institutes of the ASCR
NUMERICAL SUPPORT FOR STUDY OF STRESS RATIO EFFECT ON FATIGUE CRACK BEHAVIOUR IN THREE POINT BEND SPECIMEN MADE FROM VIBRATED CONCRETE

The fatigue behaviour of concrete has become more important for the design of structures due to more slender/slim structures, which are more sensitive to fatigue loading, or due to wind turbines, ...

Seitl, Stanislav; Thienpont, T.
Ústav fyziky materiálů, 2016

Changes in structure and phase composition in the surface of tram rail
Švábenská, Eva; Roupcová, Pavla; Schneeweiss, Oldřich
2016 - English
We have investigated structure and phase composition of surface layer of tram rails after long time running and the results were compared with those obtained on the original part of material. Changes due to effects of severe plastic deformation together with thermal shocks by friction process were expected. The information about structure and phase composition was obtained by optical and scanning electron microscopy, X-Ray Powder Diffraction, Mössbauer Spectroscopy and Glow Discharge Emission Spectroscopy (GDOES) and this was completed by microhardness measurements. The results show that the surface layer in comparison with the original material exhibits important changes in grain structure, an increase in microhardness and high content of iron oxide and hydrooxides. According to the depth profile of the chemical composition measured by GDOES there is an increase in carbon content in the surface layer which can be effect of up-hill diffusion. Keywords: tram rail; microstructure analysis; surface Available at various institutes of the ASCR
Changes in structure and phase composition in the surface of tram rail

We have investigated structure and phase composition of surface layer of tram rails after long time running and the results were compared with those obtained on the original part of material. Changes ...

Švábenská, Eva; Roupcová, Pavla; Schneeweiss, Oldřich
Ústav fyziky materiálů, 2016

HYDROGENATION OF CHOSEN MgMXN INTERMETALLICS (X=Al, Ga, In, Si, Sn)
Čermák, Jiří; Král, Lubomír; Roupcová, Pavla
2016 - English
Hydrogen sorption in chosen intermetallics MgmXn (Mg17Al12 , Mg2Ga, mixture of beta-Mg-In phases, Mg2Si and Mg2Sn) formed by magnesium and elements from the 13 th (X: Al, Ga, In) and 14 th (X: Si, Sn) groups was studied between the room temperature and T = 350 °C. Hydrogen pressure p varied from 10-3 MPa to 6 MPa.\nHydrogen solubility in alpha phase (solid solution of hydrogen in MgmXn before the hydride phase was nucleated) was close to hydrogen solubility in pure Mg. Concentration cH of hydrogen solved in Mg m X n depended linearly on pressure p ; dependence of cH on temperature T was relatively weak. MgH2 was the main hydrogen storage phase in all the compounds MgmXn . Nucleation of MgH2 at 350 °C was observed at pressure above approximately 1 MPa in Mg17Al12 and above 2 Ma in other compounds. Maximum values of c H in hydride-containing compounds MgmXn detected at T = 350 °C depended on the stability of MgmXn . Keywords: Hydrogen; hydrogen storage; Mg alloys; hydrogen solubility; MgH2 Available at various institutes of the ASCR
HYDROGENATION OF CHOSEN MgMXN INTERMETALLICS (X=Al, Ga, In, Si, Sn)

Hydrogen sorption in chosen intermetallics MgmXn (Mg17Al12 , Mg2Ga, mixture of beta-Mg-In phases, Mg2Si and Mg2Sn) formed by magnesium and elements from the 13 th (X: Al, Ga, In) and 14 th (X: Si, Sn) ...

Čermák, Jiří; Král, Lubomír; Roupcová, Pavla
Ústav fyziky materiálů, 2016

HYDROGENATION PROPERTIES OF Mg-Al-Ti-Zr-C COMPOSITE
Král, Lubomír; Čermák, Jiří; Roupcová, Pavla
2016 - English
The improvement of hydrogen storage properties of ball-milled Mg-Al-Ti-Zr-C composite was studied in this\npaper. It has been previously shown, that the addition of Ti, Zr, Al and C improves storage properties of Mg.\nThis beneficial effect of additives upon hydrogen storage properties can be explained by catalysis by the\nnanoparticles rich in Ti, Zr or Al located on the surface of Mg grains. They provide effective pathways for the\nhydrogen diffusion into the MgH2. The morphological and microstructural characteristics were investigated by\nscanning electron microscope Tescan Lyra 3 and by X-ray diffraction. The hydrogen sorption was measured\nby Sieverts method using Setaram PCT-Pro device.\nStudied experimental composite absorbed 4.2 wt.% H 2 at 573 K and 3 wt.% H 2 at 523K within 10 min. The\nhydrogen storage capacity of the composite was about 4.6% wt.% H 2 and 4.2% wt.% H 2 at 573K and 523K,\nrespectively. Keywords: Hydrides; hydrogen storage; catalysis; hydrogen; Mg-alloys Available at various institutes of the ASCR
HYDROGENATION PROPERTIES OF Mg-Al-Ti-Zr-C COMPOSITE

The improvement of hydrogen storage properties of ball-milled Mg-Al-Ti-Zr-C composite was studied in this\npaper. It has been previously shown, that the addition of Ti, Zr, Al and C improves storage ...

Král, Lubomír; Čermák, Jiří; Roupcová, Pavla
Ústav fyziky materiálů, 2016

Nanoscale phases on surface Fe-6Si magnetic sheets
Švábenská, Eva; Roupcová, Pavla; Král, Lubomír; Bulín, Tomáš; Vondráček, Martin; Foldyna, Josef; Čechal, J.; Schneeweiss, Oldřich
2016 - English
Analysis of the nanoscale phases which appear on the surface Fe-6Si samples were carried out after the various treatments – grinding and etching, annealing, and water jet abrasion. The basic information on structure, chemical and phase composition was obtained by X-Ray Powder Diffraction (XRD), Scanning Electron Microscopy with EDX, Glow Discharge Optical Emission Spectrometry (GDOES), Mössbauer Spectroscopy and X-ray Photoelectron Spectrometry (XPS). The results show high stability of the surface phase composition after the mechanical and heat treatments. Results obtained from the surface analysis in micrometer depth (XRD, EDX, GDOES) do not show any changes after the different treatments. Iron oxides were detected in XPS and conversion electron Mössbauer spectra (CEMS) which analyze the surface composition in a nanometer scale. In addition to, fine changes in atomic ordering on the surface can be observed after mechanical and heat treatments in the CEMS spectra. Keywords: Fe-Si alloy; surface modification; nanostructure Available at various institutes of the ASCR
Nanoscale phases on surface Fe-6Si magnetic sheets

Analysis of the nanoscale phases which appear on the surface Fe-6Si samples were carried out after the various treatments – grinding and etching, annealing, and water jet abrasion. The basic ...

Švábenská, Eva; Roupcová, Pavla; Král, Lubomír; Bulín, Tomáš; Vondráček, Martin; Foldyna, Josef; Čechal, J.; Schneeweiss, Oldřich
Ústav fyziky materiálů, 2016

Ab initio study of {101-2} twinning transition in magnesium
Káňa, Tomáš; Ostapovets, Andriy
2016 - English
Twinning is an important deformation mode in materials with the hexagonal close-packed (hcp) structures. The shear deformation combined with shuffling of atomic planes can lead to a transition between the Mg hcp structure and a twinned hcp structure. Studying such a transition by means of ab initio methods should bring more insight into the twinning mechanism in magnesium where the {1012} planes are the twinning planes. Comparison of ab initio results with those obtained using the semi-empirical embedded atom method is provided. It can help improve the fitted parameters of the embedded atom method. Keywords: Ab initio; Magnesium; Shear deformation Available at various institutes of the ASCR
Ab initio study of {101-2} twinning transition in magnesium

Twinning is an important deformation mode in materials with the hexagonal close-packed (hcp) structures. The shear deformation combined with shuffling of atomic planes can lead to a transition between ...

Káňa, Tomáš; Ostapovets, Andriy
Ústav fyziky materiálů, 2016

HYDROGEN ABSORPTION IN A-Co30Fe55B15
Čermák, Jiří; Král, Lubomír; Roupcová, Pavla
2016 - English
Hydrogen solved in amorphous alloys (AAs) influences their magnetic characteristics. AAs are also perspective\nas additives that can improve hydrogen storage kinetic in certain types of ball-milled hydrogen storage\nmaterials (HSMs). Therefore, knowledge of hydrogen solubility and hydrogen sorption kinetics in AAs are of a\ngreat importance for aimed design both AAs with optimal magnetic parameters and HSMs with desired sorption\ncharacteristics. In the present paper, amorphous alloy Co30Fe55B15 (an example of the type a-TM1xTM2y Bz ;\nTM - transition metal) was investigated. Hydrogen concentration c H was measured by Sieverts method in\ntemperature interval from T = 150 °C to T = 350 °C under hydrogen pressure p up to 6 MPa. It was found that\nc H was an increasing function of p and its maximum value was typically 0.5 wt.% H2 at 350 °C and 6 MPa.\nHowever, when the alloy was preliminary hydrogen charged (PHC), the pressure dependence of total c Htot in\nthe first absorption cycle(s) is non-monotonous in dependence on PHC conditions. For the sake of comparison,\nthe same absorption characteristics were measured also in Mg2Ni intermetallic that is a common constituent\nin Mg-based HSMs. Comparing Co30Fe55B15 and Mg2Ni, it was concluded that Co30Fe55B15 shows lower\nhydrogen solubility, but much better absorption kinetics. Keywords: absorption, Co 30 Fe 55 B 15; Hydrogen; Co30Fe55B15 Available at various institutes of the ASCR
HYDROGEN ABSORPTION IN A-Co30Fe55B15

Hydrogen solved in amorphous alloys (AAs) influences their magnetic characteristics. AAs are also perspective\nas additives that can improve hydrogen storage kinetic in certain types of ball-milled ...

Čermák, Jiří; Král, Lubomír; Roupcová, Pavla
Ústav fyziky materiálů, 2016

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