No (11892)
Number of found documents:
11892
Published from
to
An Enzymatic Biosensor with Amperometric Detection in a Flow Injection Analysis for the Determination of L-lactic Acid: Development and Application
Tvorynska, Sofiia; Barek, J.; Josypčuk, Bohdan
2023 - English
An amperometric biosensor consisting of an enzymatic mini-reactor (lactate oxidase covalently\nattached to −NH2 functionalized mesoporous silica powder SBA−15 using glutaraldehyde) and\na silver amalgam-based screen-printed electrode acting as a transducer was developed for the\ndetermination of L-lactic acid (LA) in FIA. The detection potential of −0.9 V vs. Ag pseudoreference\nelectrode was applied for cathodic detection of enzymatically consumed oxygen.\nUnder the optimized conditions, the constructed biosensor enabled selective determination of\nLA with a micromolar limit of detection. Importantly, the proposed biosensor represented\nexcellent operational stability after ≥350 measurements. Finally, it was successfully applied to\nreal sample analysis.
Keywords:
L-lactic acid; Lactate oxidase; Amperometric biosensor; silver amalgam
Available on request at various institutes of the ASCR
An Enzymatic Biosensor with Amperometric Detection in a Flow Injection Analysis for the Determination of L-lactic Acid: Development and Application
An amperometric biosensor consisting of an enzymatic mini-reactor (lactate oxidase covalently\nattached to −NH2 functionalized mesoporous silica powder SBA−15 using glutaraldehyde) and\na silver ...
Effect of aging on mechanical properties of 3D printed samples using stereolithography
Drechslerová, V.; Falta, J.; Fíla, T.; Dvořák, R.; Kytýř, Daniel
2023 - English
This paper focuses on stereolithography (an additive manufacturing technology working on the principle of curing liquid resins layer by layer using ultraviolet radiation) and the effect of aging on the mechanical properties of the material and printed samples. The aging of the material could be a problem for its subsequent use as the stability of the mechanical properties would not be maintained and unwanted deterioration of the material could occur. As part of the research, sets of samples were printed and subjected to different aging methods and subsequently subjected to quasi-static and dynamic uni-axial load tests. From the data obtained, the basic mechanical properties of the material were calculated and compared with each other. The aim of this paper was to investigate whether aging process causes significant changes in the mechanical properties of the materials used, which could have a consequential impact on their use in different industries.
Keywords:
stereolithography; aging; mechanical properties
Available at various institutes of the ASCR
Effect of aging on mechanical properties of 3D printed samples using stereolithography
This paper focuses on stereolithography (an additive manufacturing technology working on the principle of curing liquid resins layer by layer using ultraviolet radiation) and the effect of aging on ...
Computed tomography system with strict real-time synchronization for in-situ 3D analysis of periodically vibrating objects
Rada, Václav; Fíla, Tomáš; Zlámal, Petr; Koudelka_ml., Petr; Šleichrt, Jan; Macháček, Michael; Vavřík, Daniel; Kytýř, Daniel
2023 - English
In the contribution, we present a laboratory system capable of X-ray computed tomography (XCT) scanning of an periodically moving or oscillating object. The system is an in-house developed XCT setup with electromagnetic voice coil actuator mounted on top of the rotary stage of the setup. The strict synchronization of the components, the rotary stage, the electromagnetic actuator movement and the detector readout is accomplished with use of the detector hardware trigger and hard real-time Linux operating system. Cylindrical sample manufactured from epoxy resin with metal particles to enable movement tracking is scanned in a stationary position and during periodical movement induced by the vibration stage. The volumetric data of the scans is compared and the results of this contribution represent an important step towards identification of defects through modal analysis of in-situ harmonically vibrating object.
Keywords:
computed tomography; hardware trigger; harmonic motion; realtime synchronization
Available at various institutes of the ASCR
Computed tomography system with strict real-time synchronization for in-situ 3D analysis of periodically vibrating objects
In the contribution, we present a laboratory system capable of X-ray computed tomography (XCT) scanning of an periodically moving or oscillating object. The system is an in-house developed XCT setup ...
Nanoparticels from brake pads wear
Švábenská, Eva; Roupcová, Pavla; Friák, Martin; Schneeweiss, Oldřich
2023 - English
Exposure to particulate air pollution has been associated with a variety of health problems. One of the main\nsources of metal-rich airborne particulate pollution in roadside environments are brake-wear emissions. The \nscanning electron microscopy (SEM) and transmission electron microscopy (TEM), Mössbauer spectroscopy \n(MS), X-ray powder diffraction (XRD) was used to a make quantitative evaluation of wear particles in two \nsamples. Sizes, morphologies, oxidation state, and trace element compositions of wear particles were\ninvestigated using combination of several methods revealed high concentrations of Fe species and phases, \noften associated with carbonaceous material. SEM and TEM observations show that brake wear particles with \na size of tens to hundreds of nm mainly form particle agglomerates. However, ultrafine (<100 nm) particles are \nlikely to pose a health threat after inhalation and/or ingestion.
Keywords:
Wear particles; analysis; TEM; iron oxides; metallic particles
Available at various institutes of the ASCR
Nanoparticels from brake pads wear
Exposure to particulate air pollution has been associated with a variety of health problems. One of the main\nsources of metal-rich airborne particulate pollution in roadside environments are ...
Structural analysis of polysaccharides from mushroom hericium Erinaceus mftccb 134
Bleha, R.; Čopíková, J.; Sushytskyi, Leonid; Vannucci, Luca; Sinica, A.; Jozífek, M.; Jablonský, I.; Klouček, P.
2023 - English
The aim of this research was the structural characterisation of polysaccharides isolated from fruiting bodies of the cultivating medicinal mushroom Hericium erinaceus MFTCCB 134. Cold and hot water extracts (CWE, HWE) were obtained and purified, and followed by alkali extraction from the reminder solids. The composition and structure of the fractions were analysed by FTIR spectroscopy, and neutral sugars/linkage analyses were determined by GC/FID and GC/MS, respectively. Galactose, fucose and glucose were found in purified CWE,\nwhile glucose predominated in purified HWE.
Keywords:
Hericium erinaceus; polysaccharides; mushrooms
Available at various institutes of the ASCR
Structural analysis of polysaccharides from mushroom hericium Erinaceus mftccb 134
The aim of this research was the structural characterisation of polysaccharides isolated from fruiting bodies of the cultivating medicinal mushroom Hericium erinaceus MFTCCB 134. Cold and hot water ...
The Prager musikalisches Album (1838) and the nineteenth-century salon as cultural practice
Bunzel, Anja
2023 - English
This article deals with a collection of songs and piano pieces, the Prager musikalisches Album, published in 1838, asking two central questions. Drawing on different concepts of the musical work (Werkbegriff), I explore whether the album can be considered a work rather than a loose collection of multiple works. Within the musicological discourse there have been many attempts at defining these terms, ranging from quite narrow categorisations based on aspects of instrumentation, musical form, or stylistic matters to more open approaches encompassing the communicative process and viewing the history of genre as cultural history. Drawing on the latter, I suggest that the Prager musikalisches Album is a prime example of collective authorship, which opens up a second question, namely that of authorship. Authorship may embrace aspects of agency that exceed the realms of the person who penned a musical, literary, or artistic work. Indeed, it may be shaped by performers, audiences, presses/ salespeople, dedicatees, critics, patrons, and anyone else who has an impact on any given work at the time of its creation and/or publicization. By taking this perspective, I suggest that the Prager musikalisches Album is both reflective and representative of nineteenth-century salon culture, within whose context the album was embedded. Offering a holistic analysis of the album and its context, I use this article as a springboard to advocate for a musical historiography that takes into account the full breadth of musical culture, and which embraces, besides composers and poets, a number of other cultural agents that are often overlooked within more traditional music-historical considerations.
Keywords:
nineteenth-century salon; genre; work; Prague; authorship
Available at various institutes of the ASCR
The Prager musikalisches Album (1838) and the nineteenth-century salon as cultural practice
This article deals with a collection of songs and piano pieces, the Prager musikalisches Album, published in 1838, asking two central questions. Drawing on different concepts of the musical work ...
Analysis suggestion for vehicle scanning method
Bayer, Jan
2023 - English
An analytical approach is suggested that can be conveniently applied in the framework of the Vehicle scanning method (VSM). It assumes that the modal parameters of a bridge will be imported from a finite element (FE) program into MATLAB, where the structural response caused by a moving mass and a moving spring mass is solved using coupling equations and numerical integration. A mathematical formulation of the solution is presented together with a short numerical case study that compares the results to a traditional closed form solution. It is shown that when comparing both forms of analysis the suggested approach is more accurate in the case of slow velocities of the passing sprung mass. Other advantages are that the method allows for the mass of the vehicle or (tractor) towing vehicle and a damping \nto be included in the calculation. The user-friendly preprocessing in commercial FE programs can also be considered an advantage.
Keywords:
moving vehicle; vehicle scanning method; natural frequency; finite element analysis
Available at various institutes of the ASCR
Analysis suggestion for vehicle scanning method
An analytical approach is suggested that can be conveniently applied in the framework of the Vehicle scanning method (VSM). It assumes that the modal parameters of a bridge will be imported from a ...
A short study on self-balancing of vertical rotors mounted in passive contactless bearings
Zapoměl, Jaroslav; Kozánek, Jan
2023 - English
Energy losses and wear of the support elements of high-speed rotors can be reduced by mounting the rotors in stable passive contactless bearings, the operation of which is based on magnetic levitation. The goal of the conducted research was to investigate applicability of selfbalancing device added to vertical rotors supported by bearings showing low stiffness and damping, which is a specific property of passive magnetic bearings. This paper deals with applicability and efficiency of self-balancing devices added to vertical rotors supported by bearings having very low stiffness and damping, which corresponds to the properties of magnetic frictionless bearings.
Keywords:
self-balancing of rotors; passive contactless bearings; the influence of external damping
Available at various institutes of the ASCR
A short study on self-balancing of vertical rotors mounted in passive contactless bearings
Energy losses and wear of the support elements of high-speed rotors can be reduced by mounting the rotors in stable passive contactless bearings, the operation of which is based on magnetic ...
Dynamic tensile experiments of hard rubber on instron test machine under finite deformations
Šulc, Petr; Pešek, Luděk; Bula, Vítězslav; Šnábl, Pavel
2023 - English
This paper deals with the first experimental tests of hard rubbers under tensile harmonic loading on the axial-torsional servohydraulic Instron 8852 test machine. The objective of these experiments on cylindrical rubber specimens on this machine is to obtain stress-strain curves of rubber specimens, first considering uniaxial finite longitudinal strains for a single load cycle. Next, the hysteresis loops and their skeleton curves are compared for two selected strain measures as a function of their conjugate stress. It is shown how to obtain the dependence between elongation in the axial direction and constriction in the radial direction, which is used to determine the Cauchy stress in this configuration.
Keywords:
uniaxial harmonic loading; finite deformation; second Piola-Kirchhoff stress; hysteresis loop; Green-Lagrange strain tensor
Available at various institutes of the ASCR
Dynamic tensile experiments of hard rubber on instron test machine under finite deformations
This paper deals with the first experimental tests of hard rubbers under tensile harmonic loading on the axial-torsional servohydraulic Instron 8852 test machine. The objective of these experiments on ...
Identification of quasiperiodic processes in the vicinity of the resonance
Fischer, Cyril; Náprstek, Jiří
2023 - English
In nonlinear dynamical systems, strong quasiperiodic beating effects appear due to combination of self-excited and forced vibration. The presence of symmetric or asymmetric beatings indicates an exchange of energy between individual degrees of freedom of the model or by multiple close dominant frequencies. This effect is illustrated by the case of the van der Pol equation in the vicinity of resonance. The approximate analysis of these nonlinear effects uses the harmonic balance method and the multiple scale method.
Keywords:
dynamical systems; quasiperiodic response; van der Pol equation
Available at various institutes of the ASCR
Identification of quasiperiodic processes in the vicinity of the resonance
In nonlinear dynamical systems, strong quasiperiodic beating effects appear due to combination of self-excited and forced vibration. The presence of symmetric or asymmetric beatings indicates an ...
NRGL provides central access to information on grey literature produced in the Czech Republic in the fields of science, research and education. You can find more information about grey literature and NRGL at service web
Send your suggestions and comments to nusl@techlib.cz
Provider
Other bases