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PROPERTIES OF NANOCRYSTALLINE FE-NI PARTICLES PREPARED BY THERMAL REDUCTION OF OXALATE PRECURSORS
Švábenská, Eva; Roupcová, Pavla; Havlíček, Lubomír; Schneeweiss, Oldřich
2024 - English Recent technological advancements require development of cost-effective and high-performance magnets \nwhich ideally do not contain rare earth metals or noble metals. The promising candidates are Fe-Ni-based \nalloys, in particular, the Fe50Ni50 L10 phase (tetrataenite), which has a great perspective for producing hard \nmagnetic materials. Our study explores a promising method for preparing nanoparticles of Fe-Ni alloy from an \niron-nickel oxalate precursor. The coprecipitation method was employed to prepare oxalate precursors, \nfollowed by controlled thermal decomposition in a reducing hydrogen atmosphere. The morphology and \nproperties of the resulting particles were analysed using scanning electron microscopy (SEM) coupled with \nenergy dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD), Mössbauer spectroscopy (MS), and \nmagnetic measurements.\nThe SEM analysis revealed that the particles have approximately cube-shaped unit cell morphology with a\nsize in a range of 1 - 2 μm. Upon annealing, the samples contain multiple phases with varying Fe-Ni content.\nMagnetic measurements confirmed the formation of magnetically suitable Fe-Ni phases in the samples after \nannealing. Mössbauer spectroscopy emerged as a highly effective method for characterizing individual phases \nof the Fe-Ni system. Keywords: Magnetic materials; thermal decomposition; Mössbauer spectroscopy Available at various institutes of the ASCR PROPERTIES OF NANOCRYSTALLINE FE-NI PARTICLES PREPARED BY THERMAL REDUCTION OF OXALATE PRECURSORS

Recent technological advancements require development of cost-effective and high-performance magnets \nwhich ideally do not contain rare earth metals or noble metals. The promising candidates are ...

Švábenská, Eva; Roupcová, Pavla; Havlíček, Lubomír; Schneeweiss, Oldřich
Ústav fyziky materiálů, 2024

Modification of cooling system for laboratory measurement of rotor blade vibration
Maturkanič, Dušan; Procházka, Pavel; Hodboď, Robert; Voronova, Evgeniya; Mekhalfia, Mohammed Lamine
2024 - English Last year, the replacement of the turbine wheel model was completed in the Laboratory of Rotational Laser Vibrometry of the Institute of Thermomechanics AS CR, v.v.i. Based on previous experience and the expected higher operating load planned for the new wheel, the cooling system was modified at the same time. The paper describes the main effort in this direction and the results that clarify the previous damage of the measuring device. Keywords: blade; vibration; cooling system; measurement; laboratory Available at various institutes of the ASCR Modification of cooling system for laboratory measurement of rotor blade vibration

Last year, the replacement of the turbine wheel model was completed in the Laboratory of Rotational Laser Vibrometry of the Institute of Thermomechanics AS CR, v.v.i. Based on previous experience and ...

Maturkanič, Dušan; Procházka, Pavel; Hodboď, Robert; Voronova, Evgeniya; Mekhalfia, Mohammed Lamine
Ústav termomechaniky, 2024

Stochastic version of the arc-length method
Náprstek, Jiří; Fischer, Cyril
2024 - English The solution of a nonlinear algebraic system using the incremental method, based on pre-defined loading steps, fails in the vicinity of local extrema as well as around bifurcation points. The solution involved the derivation of the so-called ’Arc-Length’ method. Its essence lies in not incrementing the system parameter or any of the independent variables but rather the length of the response curve. The stochastic variant of this method allows for working with a system where system parameters include random imperfections. This contribution presents a variant that tracks the first two stochastic moments. Even in this simple case, interesting phenomena can be observed, such as the disappearance of the energy barrier against equilibrium jump due to random imperfections in the system. Keywords: random imperfection; stochastic arc-length method; continuation; numerical method Available in digital repository of the ASCR Stochastic version of the arc-length method

The solution of a nonlinear algebraic system using the incremental method, based on pre-defined loading steps, fails in the vicinity of local extrema as well as around bifurcation points. The solution ...

Náprstek, Jiří; Fischer, Cyril
Ústav teoretické a aplikované mechaniky, 2024

Acoustic emission methods in steel bridge degradation identification and monitoring
Šorm, Filip
2024 - English Acoustic emission methods proved to be an effective diagnostic tool in many industrial sectors. The potential of this method in the field of steel bridge diagnostics is explored in this article. The goal is to find the most effective use of this method. Keywords: steel bridges; diagnostics; acoustic emission Available in digital repository of the ASCR Acoustic emission methods in steel bridge degradation identification and monitoring

Acoustic emission methods proved to be an effective diagnostic tool in many industrial sectors. The potential of this method in the field of steel bridge diagnostics is explored in this article. The ...

Šorm, Filip
Ústav teoretické a aplikované mechaniky, 2024