No (10836)
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Výzkum zříceniny hradu Štamberk v kontextu regionu
Novotný, Jakub; Ramešová, Michaela
2023 - Czech
Příspěvek přibližuje dosavadní výsledky výzkumu hradu Štamberk realizovaného dle nově definovaných zásad pro výzkum, správu a prezentaci historických zřícenin, jehož cílem je podpořit nová řešení jak zvýšit využitelnost hradu pro cestovní ruch a integrovat památku do regionálních struktur lokalit s potenciálem cestovního ruchu. Hrad byl významným panstvím v rámci území dnešní Vysočiny. Předmětem řešení projektu, na kterém od roku 2020 spolupracuje ÚTAM AV ČR s Mikroregionem Telčsko, je výzkum historie hradu se zaměřením na technologická hlediska jeho výstavby, stavebních změn i zániku. Součástí je vytvoření 3D modelu zříceniny v krajinném kontextu. Projekt se soustředí na dějiny výroby vápna a související inventarizaci geologických lokalit. Tento výzkum přináší nové informace důležité nejen pro poznání historie hradu či pro studium analogických situací, ale také pro zvýšení atraktivity památky pro cestovní ruch. Příspěvek nejprve představí aktuální standardy výzkumu a managementu zřícenin, následně se bude zabývat nástinem potenciálu výzkumu Štamberka pro oblast cestovního ruchu s důrazem na historii hradu, mapování krajinného rámce a identifikace vazeb na regionální prostředí. Na závěr zrekapituluje dosavadní výsledky využitelné k prezentaci historického, kulturního i přírodního bohatství regionu se specifickou vazbou na cestovní ruch. The paper provides an overview of the research results of the Štamberk castle carried out according to newly defined principles for the research, management and presentation of historical ruins, the aim of which is to support new solutions to increase the usability of the castle for tourism and to integrate the monument into the regional structures of localities with tourism potential. The castle was an important place within the territory of today's Highlands. The subject of the project, on which ITAM CAS has been collaborating with the Telčsko Microregion since 2020, is research into the history of the castle with a focus on the technological aspects of its construction, structural changes and demise. It includes the creation of a 3D model of the ruins in a landscape context. The project focuses on the history of lime production and the related inventory of geological sites. This research brings new information important not only for learning about the history of the castle or for studying analogous situations, but also for increasing the attractiveness of the monument for tourism. The paper first presents the current standards of research and management of ruins, then it deals with an outline of the research potential of Štamberk for the field of tourism with an emphasis on the history of the castle, mapping the landscape framework and identifying links to the regional environment. At the end, it summarizes the results so far that can be used to present the historical, cultural and natural wealth of the region with a specific link to tourism.
Keywords:
Štamberk; ruin; technological research; presentation of monuments; tourism
Available at various institutes of the ASCR
Výzkum zříceniny hradu Štamberk v kontextu regionu
Příspěvek přibližuje dosavadní výsledky výzkumu hradu Štamberk realizovaného dle nově definovaných zásad pro výzkum, správu a prezentaci historických zřícenin, jehož cílem je podpořit nová řešení jak ...
Adaptation of methods for cyclo-stationary processes for noisy structural health data
Fischer, Cyril; Bayer, Jan; Náprstek, Jiří; Urushadze, Shota
2023 - English
In structural health analysis, various techniques, including indirect measurement via monitoring vehicles, often yield data with significant randomness and insufficient frequency separation. Conversely, the desired attributes under scrutiny are periodic in nature. Thus, methodologies designed to identify cyclo-stationary properties within noisy data can be adapted for such scenarios, assuming an adequate length of the recorded data.
Keywords:
data analysis; cyclo-stationary processes; structural health monitoring
Available at various institutes of the ASCR
Adaptation of methods for cyclo-stationary processes for noisy structural health data
In structural health analysis, various techniques, including indirect measurement via monitoring vehicles, often yield data with significant randomness and insufficient frequency separation. ...
Consistency of mathematical and experimental model of the autoparametric system
Fischer, Cyril; Náprstek, Jiří
2023 - English
This paper presents a long-overdue comparison of data obtained from experimental investigation of a spherical vibration absorber with the results of two mathematical models of the motion of a heavy sphere in a spherical surface. It shows that the danger posed by the potentially unstable self-parametric nature of the mathematical system is not too great in the case of realistic configurations, and that the values of the parameters describing the realistic structures remain within intervals corresponding to the stable behaviour of the absorber.
Keywords:
vibration absorber; rolling sphere; spherical surface; autoparametric system; structural health monitoring
Available at various institutes of the ASCR
Consistency of mathematical and experimental model of the autoparametric system
This paper presents a long-overdue comparison of data obtained from experimental investigation of a spherical vibration absorber with the results of two mathematical models of the motion of a heavy ...
Laserová ablace atomů vápníku a hliníku jako zdroj částic pro iontovou past
Grim, Jakub; Pekař, Zdeněk; Pham, Minh Tuan; Číp, Ondřej
2023 - Czech
Laserová ablace je účinnou metodou pro generování částic z různých materiálů, včetně těch s vysokou teplotou vypařování, jako je hliník. Využití vysokoenergetických laserových pulsů umožňuje kontrolované odpaření materiálu a vytvoření ablačního kráteru. V pilotní sestavě pro generování neutrálních atomů vápníku a hliníku pomocí laserové ablace byly dosaženy úspěšné výsledky. Metoda je porovnávána s tepelnou píckou s cílem optimalizovat proces generování těchto částic. Následná spektroskopická měření na generovaných atomech jsou prováděna s cílem optimalizace absorpce a emise fotonů pro následnou ionizaci v iontové pasti. Studie přechodů neutrálních atomů Ca a Al ukazuje, že laserová ablace poskytuje efektivnější generaci atomů s možností větší kontroly nad tímto procesem. Laser ablation is an effective method for generating particles from a variety of materials, including those with high evaporation temperatures such as aluminum. The use of high-energy laser pulses enables controlled evaporation of the material and the creation of an ablation crater. Successful results have been obtained in a pilot setup for the generation of neutral calcium and aluminium atoms by laser ablation. The method is being compared with thermal resistance oven in order to optimize the prosec generation of these particles. Subsequent spectroscopic measurements on the generated atoms are performed to optimize the absorption and emission of photons for subsequent ionization in the ion trap. A study of the transitions of neutral Ca and Al atoms shows that laser ablation provides a more efficient generation of atoms with the possibility of greater control over the process.
Keywords:
laser ablation; ion trap; particle generation; fluorescence spectroscopy
Available at various institutes of the ASCR
Laserová ablace atomů vápníku a hliníku jako zdroj částic pro iontovou past
Laserová ablace je účinnou metodou pro generování částic z různých materiálů, včetně těch s vysokou teplotou vypařování, jako je hliník. Využití vysokoenergetických laserových pulsů umožňuje ...
Comparison of finite element simulation of tungsten nanoindentation with Berkovich and conical indenter
Fiala, L.; Ballo, I.; Kovář, J.; Fuis, Vladimír
2023 - English
Finite Element Method (FEM) was used to study the difference between using Berkovich and conical indenters in nanoindentation test of tungsten specimen. The study was aimed to determine the\nmodulus of elasticity of a tested specimen and how it changes with different indenter. The FEM analysis also revealed that the modulus of elasticity was sensitive to the dimensions of both specimen and the indenter for which were made several numerical calculations with different dimensions.
Keywords:
nanoindentation; FEM; Berkovich indenter; conical indenter; tungsten
Available at various institutes of the ASCR
Comparison of finite element simulation of tungsten nanoindentation with Berkovich and conical indenter
Finite Element Method (FEM) was used to study the difference between using Berkovich and conical indenters in nanoindentation test of tungsten specimen. The study was aimed to determine the\nmodulus ...
Analýza sekundárních metabolitů streptomycet Ramanovou spektroskopií in vivo
Mikulová, Adéla; Petříčková, K.; Bobek, J.; Chroňáková, Alica; Samek, Ota; Pilát, Zdeněk
2023 - Czech
Práce se zabývá studiem Ramanových spekter sekundárních metabolitů bakterií rodu Streptomyces, zejména polyenních antifungálních látek. Purifikované izoláty a komerční standardy těchto sloučenin byly využity k pořízení referenčních spekter, ze kterých byly odvozeny spektrální markery charakterizující konkrétní detaily chemické struktury. Verifikace pozorovaných markerů byla provedena pomocí predikcí Ramanových spekter in silico. Následně byly tyto poznatky využity ke spektroskopické charakterizaci složení sekundárních metabolitů in vivo, přímo v bakteriích rostoucích na pevném médiu. Vypracované metodiky pomohou optimalizovat podmínky pro biotechnologickou produkci antibiotik. The work deals with the study of Raman spectra of secondary metabolites of bacteria of the genus Streptomyces, especially polyene antifungal agents. Purified isolates and commercial standards of these compounds were used to obtain reference spectra from which spectral markers characterizing specific details of the chemical structure were derived. Verification of the observed markers was performed using in silico Raman spectra predictions. Subsequently, these findings were used for the spectroscopic characterization of the composition of secondary metabolites in vivo, directly in bacteria growing on a solid medium. The developed methodologies will help to optimize the conditions for the biotechnological production of antibiotics.
Keywords:
Raman spectroscopy; microbiology; Streptomyces; antibiotics
Available at various institutes of the ASCR
Analýza sekundárních metabolitů streptomycet Ramanovou spektroskopií in vivo
Práce se zabývá studiem Ramanových spekter sekundárních metabolitů bakterií rodu Streptomyces, zejména polyenních antifungálních látek. Purifikované izoláty a komerční standardy těchto sloučenin byly ...
Mechanical properties of basalt: a study on compressive loading at different strain rates using SHPB
Falta, J.; Krčmářová, N.; Fíla, T.; Vavro, Martin; Vavro, Leona
2023 - English
This article focuses on the mechanical properties of basalt in compressive loading at different strain-rates. The study employs advanced instrumentation for the evaluation of the results in dynamic conditions, while standard uni-axial loading device is used for evaluation in quasi-static conditions. Basalt specimens were subjected to four different loading-rates from 200–600 s−1 on which the stress-strain dependence was evaluated together with DIC analysis of crack initiation and disintegration process. Understanding the mechanical properties of basalt can provide insights for engineers and designers in creating structures that are durable and able to withstand different loading conditions. The findings of this study can have implications for a wide range of industries, including aerospace, automotive, and construction, among others.
Keywords:
SHPB; basalt; compressive loading; dynamic loading
Available at various institutes of the ASCR
Mechanical properties of basalt: a study on compressive loading at different strain rates using SHPB
This article focuses on the mechanical properties of basalt in compressive loading at different strain-rates. The study employs advanced instrumentation for the evaluation of the results in dynamic ...
Asynchronous time integration while achieving zero interface energy
Dvořák, Radim; Kolman, Radek; Falta, J.; Neühauserová, M.
2023 - English
This contribution deals with an asynchronous direct time integration of the finite-element model. The proposed method is applied to the phenomenon of wave propagation through an elastic linear continuum. The numerical model is partitioned into individual subdomains using the domain decomposition method by means of localized Lagrange multipliers. For each subdomain, different time discretizations are used. No restrictions for relation between subdomain’s time steps are imposed. The coupling of the subdomains is forced by an acceleration continuity condition. Additionally, we use the a posteriori technique to also provide the displacement and velocity continuity at the interfaces, and hence we obtain exact continuity of all three kinematic fields. The proposed method is experimentally validated using the modified SHPB (split Hopkinson pressure bar) setup.
Keywords:
finite element method; direct time integration; asynchronous integration; domain decomposition; localized lagrange multipliers
Available at various institutes of the ASCR
Asynchronous time integration while achieving zero interface energy
This contribution deals with an asynchronous direct time integration of the finite-element model. The proposed method is applied to the phenomenon of wave propagation through an elastic linear ...
Soustava frekvenčních normálů na ÚPT
Čížek, Martin; Hrabina, Jan; Pravdová, Lenka; Číp, Ondřej
2023 - Czech
Příspěvek představuje systém frekvenčních normálů vyvinutý na Ústavu přístrojové techniky AVČR. Diskutuje potřebu vysoce koherentních optických frekvenčních referencí pro náročné experimenty v spektroskopii se zchlazenými atomy. Systém zahrnuje propojené normály pracující v rádiové a optické části elektromagnetického spektra, včetně aktivního vodíkového maseru, vláknového laseru uzamčeného na vysoce jakostní optický rezonátor a optického frekvenčního hřebene. Relativní frekvenční stabilita těchto normálů je analyzována s důrazem na jejich vhodnost pro různé integrační časy a aplikace. Dále je popsáno experimentální uspořádání pro porovnání stability frekvenčních normálů na ÚPT s těmi v laboratoři BEV ve Vídni pomocí stabilizované fázově koherentní optické vláknové linky. Výsledky ukazují vynikající relativní stabilitu frekvenčních normálů dosahující -15. řádu, která je nezbytná pro aplikace ve spektroskopii a experimenty se zachycenými zchlazenými ionty. The contribution presents a system of frequency standards developed at the Institute of Scientific Instruments of the Czech Academy of Sciences. It discusses the need for highly coherent optical frequency references for demanding experiments in spectroscopy with cooled atoms. The system comprises interconnected standards operating in the radiofrequency and optical parts of the electromagnetic spectrum, including an active hydrogen maser, a fiber laser locked to a high-finesse optical resonator, and an optical frequency comb. The relative frequency stability of these standards is analyzed, highlighting their suitability for different integration times and applications. The article also describes the experimental setup for comparing the stability of the frequency standards at the Institute of Scientific Instruments with those at the BEV laboratory in Vienna using a stabilized phase-coherent optical fiber link. The results demonstrate the excellent stability of the frequency standards reaching the -15th order of magnitude, essential for spectroscopy and ion trapping experiments.
Keywords:
time and frequency standards; photonic networks; measurement of optical frequency stability
Available at various institutes of the ASCR
Soustava frekvenčních normálů na ÚPT
Příspěvek představuje systém frekvenčních normálů vyvinutý na Ústavu přístrojové techniky AVČR. Diskutuje potřebu vysoce koherentních optických frekvenčních referencí pro náročné experimenty v ...
NANOCERIA PREPARED BY ELECTRON BEAM EVAPORATION
Pizúrová, Naděžda; Hlaváček, Antonín; Kavčiaková, Zuzana; Roupcová, Pavla; Kuběna, Ivo; Buršík, Jiří; Sokovnin, S. Y.
2023 - English
Cerium oxide nanoparticles (nanoceria) are currently one of the most investigated nanomaterials because of their attractive properties used in biomedical applications, catalysis, fuel cells, and many others. These attractive properties are connected with the Ce3+ and Ce4+ valency state ratio. In the nanoparticle form, cerium oxides contain a mixture of Ce3+ and Ce4+ on the nanoparticle surfaces. Switching between these two states requires oxygen vacancies. Therefore, nanoceria's inherent ability to act as an antioxidant in an environmentally-dependent manner and a “redox switch” to confer auto-regenerating capabilities by automatically shifting between Ce4+ and Ce3+ oxidation states is significantly affected by surface morphology. Regarding this demanded behavior, we aimed to characterize synthesized nanoparticle surface quality and its influence on the cerium oxidation states. The received results were used to evaluate the synthesis method's suitability for suggested utilization. We used nanoparticles prepared by electron beam evaporation. This unique physical method includes nanoparticle creation through the fast cooling process followed by breaking radiation damaging nanoparticle surfaces to create surface off-stoichiometry. We prepared a sample containing clusters of a mixture of ultra-small nanoparticles and approximately 100 nm particles. X-ray diffraction confirmed the CeO2 phase in both components. To extract the finest component, we used centrifugal size fractionation. We received 200 nm clusters of 2-10 nm nanoparticles. Nanoparticle shapes and facet types were analyzed using transmission electron microscopy methods. We found out most nanoparticles were formed with truncated octahedrons containing {1,1,1} and {1,0,0} facet types and truncated cuboctahedrons containing {1,1,1}, {1,0,0}, and additional {1,1,0} facets. No octahedron (without truncation) containing only {1,1,1} facets was observed. Nanoparticle shapes containing {1,1,0} and {1,0,0} are suitable for redox activity. Some amount of irregular shapes, beneficial for redox activity, was also observed. Spectroscopy methods confirmed Ce3+ content.
Keywords:
Ce3+ and Ce4+; electron beam evaporation; facet types; hrtem; Nanoceria
Available at various institutes of the ASCR
NANOCERIA PREPARED BY ELECTRON BEAM EVAPORATION
Cerium oxide nanoparticles (nanoceria) are currently one of the most investigated nanomaterials because of their attractive properties used in biomedical applications, catalysis, fuel cells, and many ...
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