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Generování hydridů ve spojení s hmotnostní spektrometrií s indukčně vázaným plazmatem
Matoušek, Tomáš
2019 - Czech
Přehledný text popisující využití techniky generování těkavých hydridů v hmotnostní spektrometrií s indukčně vázaným plazmatem včetně speciačních analýz. An overview describing technique of volatile hydride generation in connection with inductively coupled plasma mass spectrometry including speciation analysis.
Keywords:
hydride generation; ICP-MS; speciation analysis
Available at various institutes of the ASCR
Generování hydridů ve spojení s hmotnostní spektrometrií s indukčně vázaným plazmatem
Přehledný text popisující využití techniky generování těkavých hydridů v hmotnostní spektrometrií s indukčně vázaným plazmatem včetně speciačních analýz....
NMR Metabolomics Study of the Association between Pancreatic Cancer and Diabetes Mellrtus.
Michálková, Lenka; Horník, Štěpán; Sýkora, Jan; Habartová, L.; Setnička, V.
2019 - English
In our study, 1H NMR metabolomics was employed to plasma samples of pancreatic cancer patients, individuals with long-term diabetes mellitus type 2 (lasting more than 5 years) and healthy controls. The NMR analyses were followed by establishing a statistical model based on principal component analysis and discriminant analysis. The aim was to discover differences between these groups and to define a potential biomarker panel. The statistical evaluation of metabolomics-based profiles provided high values of sensitivity and specificity. Subsequently, plasma samples of the risk group, specifically patients with recently diagnosed diabetes mellitus with a duration of <3 years (possible T3cDM), were analysed and the possibility of PC development was predicted. The achieved results showed strong potential of 1H NMR metabolomics to establish a biomarker panel that would facilitate the early diagnosis of PC and the possibility identify diabetic individuals, who are at risk of developing PC.
Keywords:
pancreatic cancer; nmr analyses; biomarker panel
Available in a digital repository NRGL
NMR Metabolomics Study of the Association between Pancreatic Cancer and Diabetes Mellrtus.
In our study, 1H NMR metabolomics was employed to plasma samples of pancreatic cancer patients, individuals with long-term diabetes mellitus type 2 (lasting more than 5 years) and healthy controls. ...
Dialytic Separation of Anions from DMSO Solution Facilitated by dendritic Receptors.
Cuřínová, Petra; Winkler, Maximilian; Krupková, Alena; Budka, J.; Wun, Ch.N.; Blechta, Vratislav; Červenková Šťastná, Lucie; Sýkora, Jan; Strašák, Tomáš
2019 - English
As the dialytic tubing is impermeable for big molecules of receptor, the anions crossing the barrier of dialytic tubing to form complex with the receptor stay entrapped inside and can be removed from the solution. NMR methods were used to study the complexation properties of given receptors as well as to determine the concentration changes during dialytic experiments.
Keywords:
anions; receptor; dialytic experiments
Available in a digital repository NRGL
Dialytic Separation of Anions from DMSO Solution Facilitated by dendritic Receptors.
As the dialytic tubing is impermeable for big molecules of receptor, the anions crossing the barrier of dialytic tubing to form complex with the receptor stay entrapped inside and can be removed from ...
Stanovení rychlých změn koncentrací těkavých organických sloučenin pomocí difúzního denuderu
Křůmal, Kamil; Mikuška, Pavel
2019 - Czech
Stanovení rychlých změn koncentrací těkavých organických sloučenin bylo provedeno využitím difúzního denuderu se stékajícím filmem kapaliny, který umožňuje odběr vzorků v časových intervalech již od 2 minut. Determination of fast changes in concentrations of volatile organic compounds was performed using wet effluent diffusion denuder, which allows collection of samples in 2-min intervals.
Keywords:
monoterpenes; BTEX; denuder
Available in digital repository of the ASCR
Stanovení rychlých změn koncentrací těkavých organických sloučenin pomocí difúzního denuderu
Stanovení rychlých změn koncentrací těkavých organických sloučenin bylo provedeno využitím difúzního denuderu se stékajícím filmem kapaliny, který umožňuje odběr vzorků v časových intervalech již od 2 ...
Influence of Surface Treatment of Thin-Film Composite Membrane on Separation of Carbon Dioxide from Biogas.
Morávková, Lenka; Kárászová, Magda; Petrusová, Zuzana; Izák, Pavel
2019 - English
The effect of the various wetting procedure on the membrane performance was studied [1]. Spraying is clearly more efficient than spreading water on the top of the membrane with a brush and results in higher methane purity. Spraying ensures a more uniform distribution of the water on the skin layer of the membrane, leading to much higher CO2 permeation through the membrane and higher CH4 content in the retentate stream.
Keywords:
biogas; separation; carbon dioxide
Available in a digital repository NRGL
Influence of Surface Treatment of Thin-Film Composite Membrane on Separation of Carbon Dioxide from Biogas.
The effect of the various wetting procedure on the membrane performance was studied [1]. Spraying is clearly more efficient than spreading water on the top of the membrane with a brush and results in ...
Magnesium Silicide and Germanide from Electronic Waste as a Source of CVD Precursors for Potential Catalysts Preparation.
Bumba, Jakub
2019 - English
This work is focused on the regeneration of silicon and germanium from electronic waste and on the possibility of intermediate products utilization e.g. for chemical vapour deposition (CVD) and catalysis.
Keywords:
electronic waste; silicon and germanium; catalysts preparation
Available in a digital repository NRGL
Magnesium Silicide and Germanide from Electronic Waste as a Source of CVD Precursors for Potential Catalysts Preparation.
This work is focused on the regeneration of silicon and germanium from electronic waste and on the possibility of intermediate products utilization e.g. for chemical vapour deposition (CVD) and ...
Five Years of Aerosol Particles Growth Rate Measurements at Four Background Stations in the Czech Republic.
Holubová Šmejkalová, Adéla
2019 - English
In this work we used data on aerosol particle number size distribution to investigate if there are any differences or similarities in the growth rate at four background stations located in different types of environment (urban, industrial, agricultural and suburban).
Keywords:
atmospheric aerosols; model simulations; background stations
Available in a digital repository NRGL
Five Years of Aerosol Particles Growth Rate Measurements at Four Background Stations in the Czech Republic.
In this work we used data on aerosol particle number size distribution to investigate if there are any differences or similarities in the growth rate at four background stations located in different ...
Synthetic Pathways Leading to Phosphahelicenes.
Beránek, Tomáš
2019 - English
The goal of this work is to explore possible synthetic ways leading to these new members of the helicene family.\n
Keywords:
sythetic way; phosphorus; helicenes
Available in a digital repository NRGL
Synthetic Pathways Leading to Phosphahelicenes.
The goal of this work is to explore possible synthetic ways leading to these new members of the helicene family.\n
Voltametrické stanovení pálivosti chilli paprik na elektrodě ze skelného uhlíku modifikované fosfolipidy
Skopalová, J.; Rajcová, A.; Vokounová, D.; Navrátil, Tomáš
2019 - Czech
Kapsaicin je přírodní alkaloid vyskytující se v plodech chilli paprik, které patří k nejdůležitějším a nejrozšířenějším kořením. Za jejich popularitou stojí významné organoleptické vlastnosti (typická pálivá chuť), antioxidační či antimikrobiální účinky. Pálivost chilli paprik je hlavním důvodem jejich konzumace a z pohledu konzumenta představuje jednu z jejich nejdůležitějších charakteristik. Od toho se proto odvozuje potřeba tuto charakteristiku kvantifikovat. Míra pálivosti přímo souvisí s obsahem kapsaicinu a jemu podobných látek (kapsaicinoidů) v paprikách. Kromě potravinářství nachází kapsaicin své užití i v lesnictví (zemědělství) jako ochrana před okusem stromů zvěří. The aim of this study was to develop a simple method for evaluation of the pungency in chili peppers with a glassy carbon electrode modified using phospholipid membrane prepared from asolectin. For these purposes cyclic voltammetry (CV) and differential pulse voltammetry (DPV) have been used. A few different methods have been tested: direct method, transfer method on unmodified and modified electrode, using standard addition method as well as calibration curve method. A statistically significant correlations with the results of the reference HPLC method have been found in case of voltammetric methods, especially in DPV with asolectin modified electrode.
Keywords:
capsaicin; voltammetry; glassy carbon electrode
Available on request at various institutes of the ASCR
Voltametrické stanovení pálivosti chilli paprik na elektrodě ze skelného uhlíku modifikované fosfolipidy
Kapsaicin je přírodní alkaloid vyskytující se v plodech chilli paprik, které patří k nejdůležitějším a nejrozšířenějším kořením. Za jejich popularitou stojí významné organoleptické vlastnosti (typická ...
Hydrotreating over Silica-Alumina Supported Catalysts
Gulková, Daniela; Vít, Zdeněk; Kaluža, Luděk
2019 - English
They are studied for possible use in deep hydrodesulfurization (HDS)1 while they have not been investigated for the HDS parallel with hydrodeoxygenation (HDO)2. The aim was to find the effect of active phase and support of Pd and PdPt catalysts on activity and selectivity in HDS of 4,6-dimethyldibenzothiophene (DMDBT) and HDS/HDO of l-benzothiophene/octanoic acid (BT/OA).
Keywords:
catalysts; silica-alumina; hydrodesulfurization
Available in a digital repository NRGL
Hydrotreating over Silica-Alumina Supported Catalysts
They are studied for possible use in deep hydrodesulfurization (HDS)1 while they have not been investigated for the HDS parallel with hydrodeoxygenation (HDO)2. The aim was to find the effect of ...
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