No (235)
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235
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Modelling of non-monotonous course of shear viscosity
Filip, Petr
2018 - English
A number of parameters appearing in the 'classical' empirical constitutive equations usually oscillate between two and five. With the onset of new rheologically more complex materials exhibiting non-monotonous behaviour of flow curves this range (2-5) is no longer tenable and more additional parameters are required for a proper description of the flow curves. An 8-parameter model is presented and testified.
Keywords:
viscosity; flow curve; constitutive equation; empirical modelling
Available at various institutes of the ASCR
Modelling of non-monotonous course of shear viscosity
A number of parameters appearing in the 'classical' empirical constitutive equations usually oscillate between two and five. With the onset of new rheologically more complex materials exhibiting ...
The role of solvents in the preparation of hydrophobic nanofibrous membrane containing fumed silica
Peer, Petra; Polášková, M.; Musilová, I.; Filip, Petr
2018 - English
It is well-known that a type of used fumed silica nanoparticles plays a dominant role in wettability of the corresponding nanofibrous mats. As a result, the desired contact angle can be approximately achieved by a choice of adequate fumed silica nanoparticles. However, less attention has been hitherto paid to an active role of solvents in connection with the tailoring this contact angle. For analysis we used poly(vinyl butyral) representing electrospun-friendly material, various types of fumed silica nanoparticles and two solvents - methanol and ethanol. It is demonstrated that a choice of polymer solvents plays a significant role in contact angle changes. Hence, in combination of the type of fumed silica nanoparticles and the type of solvent it is possible to achieve a finer partition of the required contact angles.
Keywords:
PVB solution; solvents; fumed silica; electrospinning; rheology
Available at various institutes of the ASCR
The role of solvents in the preparation of hydrophobic nanofibrous membrane containing fumed silica
It is well-known that a type of used fumed silica nanoparticles plays a dominant role in wettability of the corresponding nanofibrous mats. As a result, the desired contact angle can be approximately ...
Thermal induced morphological changes of poly(ethylene oxide) nanofibrous webs
Polášková, M.; Peer, Petra; Ponížil, P.; Čermák, R.
2018 - English
The crystallinity of fibres prepared by electrospinning shows lower level in comparison with samples processed by common technologies such as moulding or film casting. Thus, the attempts to improve the structure of electrospun fibres in order to increase physical and mechanical properties of nonwoven webs are obvious. Post-process thermal treatment is one of the possibilities of the crystallinity enhancement that can be easily included to the finishing operation of final products. For the experiment we used poly(ethylene oxide) representing electrospun-friendly material and two solvents - methanol and water, both ensuring good electrospinnability. It is demonstrated that a choice of polymer solvents plays a significant role in fibre diameter and their capabilities to resist applied heat. However, in all cases the enhancement of crystallinity is detected at the short time of thermal exposure.
Keywords:
PEO nanofibres; degree of crystallinity; electrospinning
Available at various institutes of the ASCR
Thermal induced morphological changes of poly(ethylene oxide) nanofibrous webs
The crystallinity of fibres prepared by electrospinning shows lower level in comparison with samples processed by common technologies such as moulding or film casting. Thus, the attempts to improve ...
Image analysis of particle size: effect of light source type
Formánek, R.; Kysela, Bohuš; Šulc, R.
2018 - English
Agitation of two immiscible liquids or solid-liquid suspension is a frequent operation in chemical and metallurgical industries. The sizes of particles, bubbles or droplets can be determined by the Image Analysis Technique. It is known that the quality of captured images depends significantly on the original image background that is mainly affected by the type of the light source. The aim of this contribution is to investigate the effect of light source type on image quality. The four types of light sources were tested: 1) 1000 W halogen lamp, 2) 72 W LED bar panel, 3) 60 W LED chip, and 4) 90 W LED chip. The illumination intensity and image background quality were investigated for each tested light sources. The effect of the shutter speed on evaluated particle sizes was tested using monodisperse spherical calibration particles having diameter of 1.19 mm. The difference observed between particle sizes evaluated by image analysis for given light source and declared calibration particle diameter was used as a measure of light source quality.
Available at various institutes of the ASCR
Image analysis of particle size: effect of light source type
Agitation of two immiscible liquids or solid-liquid suspension is a frequent operation in chemical and metallurgical industries. The sizes of particles, bubbles or droplets can be determined by the ...
Settling slurry flow near deposition velocity in inclined pipe of negative slope
Kesely, Mikoláš; Matoušek, Václav; Vlasák, Pavel
2018 - English
Pipe flow of sand-water slurry (settling slurry) is sensitive to pipe inclination. The effect of the angle to which the partially stratified flow is inclined from the horizontal has been subject to investigation in numerous studies. However, almost all of them focus on ascending flows, i.e. flows inclined to positive angles of inclination. It is well known that settling slurry flows inclined to negative slopes (descending flows) differ from those inclined to positive slopes, particularly at velocities near the deposition limit. The deposition limit velocity is the flow velocity at which stationary deposit starts to be formed at the bottom of the pipe. We investigate the effect of the negative slope on pipe flow near deposition limit velocity in the broad range of inclination angles. Besides the deposition limit, we focus on the distribution of solids across the pipe cross section. We combine experimental approach with mathematical modelling. Our new experiments with medium-to-coarse sand (mass-medium grain size 0.87 mm) in a 100-mm pipe inclined from 0 to -45 degree provide suitable data for a validation of predictions of our layered model for partially stratified flows in inclined pipes.
Available at various institutes of the ASCR
Settling slurry flow near deposition velocity in inclined pipe of negative slope
Pipe flow of sand-water slurry (settling slurry) is sensitive to pipe inclination. The effect of the angle to which the partially stratified flow is inclined from the horizontal has been subject to ...
Effect of pipe inclination on flow behaviour of fine-grained settling slurry
Vlasák, Pavel; Chára, Zdeněk; Matoušek, Václav; Konfršt, Jiří; Kesely, Mikoláš
2018 - English
The effect of flow parameters of fine-grained settling slurry on the pressure drop-velocity relationship, deposition limit velocity and local concentration distribution was studied in an experimental pipe loop of inner diameter D = 100 mm with inclinable pipe sections for pipe inclination ranging from – 45° to +45°. The slurry consisted from water and narrow particle size distribution glass beads of mean diameter d50 = 0.18 mm. The concentration distribution was studied with application of a gamma-ray densitometry. The deposition velocity was defined as the flow velocity at which stationary deposit started to be formed at the pipe invert. The study revealed the stratified flow pattern of the studied slurry in inclined pipe sections, for slurry velocities below to the deposition limit sliding or stationary bed were created in ascending pipe sections. For low pipe inclination ( < ± 25°) the effect of inclination on local concentration distribution was not significant. Mean transport concentration for descending flow was lower than that for the ascending flow Deposition limit in inclined pipe was slightly lower than that in horizontal pipe. Frictional pressure drops in ascending pipe were higher than that in descending pipe, the difference decreased with increasing velocity and inclination.
Available at various institutes of the ASCR
Effect of pipe inclination on flow behaviour of fine-grained settling slurry
The effect of flow parameters of fine-grained settling slurry on the pressure drop-velocity relationship, deposition limit velocity and local concentration distribution was studied in an experimental ...
Turbulence characteristics scaling in Rushton turbine impeller discharge flow: effect of PIV system setup
Šulc, R.; Ditl, P.; Fořt, I.; Jašíková, D.; Kotek, M.; Kopecký, V.; Kysela, Bohuš
2018 - English
Study of mechanism of turbulent energy dissipation rate in the impeller discharge stream from a standard Rushhton turbine impeler in a model cylyndrical vessel with radial baffles.
Available at various institutes of the ASCR
Turbulence characteristics scaling in Rushton turbine impeller discharge flow: effect of PIV system setup
Study of mechanism of turbulent energy dissipation rate in the impeller discharge stream from a standard Rushhton turbine impeler in a model cylyndrical vessel with radial baffles.
Experimental investigation of settling slurry flow in inclined pipe sections
Vlasák, Pavel; Chára, Zdeněk; Matoušek, Václav; Kesely, Mikoláš; Konfršt, Jiří
2018 - English
Narrow particle size distribution glass beads-water slurry flow in the pipe sections of different inclination were investigated on an experimental pipe loop of inner diameter D = 100 mm. The study refers to the effect of pipe inclination and slurry velicity on local concentration distribution, pressure drop-velocity relationship, and deposition limit. The study revealed that the glass beads-water mixtures in the inclined pipe sections were significantly stratified: the solid particles moved principally close to the pipe invert, and for flow velocities close to the deposition limit sliding bed or stationary deposit is created even in inclined pipe sections.
Keywords:
settling slurry; inclined pipe; pressure drops; concentration distribution; radiometry
Available at various institutes of the ASCR
Experimental investigation of settling slurry flow in inclined pipe sections
Narrow particle size distribution glass beads-water slurry flow in the pipe sections of different inclination were investigated on an experimental pipe loop of inner diameter D = 100 mm. The study ...
Dependence of morphology of electrospun PVB nanofibres containing fumed silica on elasticity of the processed solutions
Peer, Petra; Polášková, M.; Filip, Petr
2017 - English
Application of various types of fumed silica gives a possibility to tailor a degree of hydrophilicity or hydrophobicity of the resulting electrospun nanofibrous mats where as a basic polymeric material is taken poly(vinyl butyral) (PVB) solved in methanol. Presence of fumed silica substantially changes viscoelastic attributes in comparison with the neat PVB solution.\nThe aim of this contribution is to compare morphological structures of the resulting electrospun mats generated from the solutions with presence and absence of various types of fumed silica differing in surface morphology, size and the specific surface area. This comparison is based on the rheological characteristics with the emphasis to elasticity of the pre-processed solutions. The differences in elasticity among fumed silica based solutions are indeed remarkable. The obtained results show that elasticity does not play a crucial role in creation and morphological aspects of the corresponding nanofibrous mats including fibres diameter.
Keywords:
rheology; elasticity; PVB solution; fumed silica; electrospinning
Available at various institutes of the ASCR
Dependence of morphology of electrospun PVB nanofibres containing fumed silica on elasticity of the processed solutions
Application of various types of fumed silica gives a possibility to tailor a degree of hydrophilicity or hydrophobicity of the resulting electrospun nanofibrous mats where as a basic polymeric ...
Flow behaviour and structure of heterogeneous particles-water mixture in horizontal and inclined pipes
Vlasák, Pavel; Chára, Zdeněk; Konfršt, Jiří
2017 - English
Available at various institutes of the ASCR
Flow behaviour and structure of heterogeneous particles-water mixture in horizontal and inclined pipes
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