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ENHANCING WELD JOINT INTEGRITY IN S460 HIGH-STRENGTH STEEL PLATES: AN EXPERIMENTAL APPROACH
Al Khazali, Mohammad Sami; Malíková, Lucie; Křivý, V.; Seitl, Stanislav
2024 - anglický
Exploring S460 steel, this research assesses weld toe microstructure and fatigue. It finds that welding affects \nhardness of welded area and fatigue life. These insights are crucial for structural engineering, optimizing welding \npractices for longevity. \nTests confirm increased weld toe hardness correlates with fatigue resistance. This informs design strategies, \nensuring bridge safety under cyclic loads. The study advances understanding of HSS behaviour, influencing future \nwelding techniques.
Klíčová slova:
High-strength steel; weld's toe; cruciform joints; S460; fatigue behaviour
Plné texty jsou dostupné na jednotlivých ústavech Akademie věd ČR.
ENHANCING WELD JOINT INTEGRITY IN S460 HIGH-STRENGTH STEEL PLATES: AN EXPERIMENTAL APPROACH
Exploring S460 steel, this research assesses weld toe microstructure and fatigue. It finds that welding affects \nhardness of welded area and fatigue life. These insights are crucial for structural ...
Correlative probe electron microscopy analysis of plasma-treated gallium-doped zinc oxide nanorods
Rutherford, D.; Remeš, Zdeněk; Mičová, J.; Ukraintsev, E.; Rezek, B.
2024 - anglický
Correlative Probe Electron Microscopy (CPEM) was used to investigate the topographical and electronic emission properties of gallium-doped zinc oxide nanorods (ZnO:Ga) after low pressure hydrogen or oxygen plasma treatment. Simultaneous secondary electron (SE) and back-scattered electron (BSE) emission information from the same nanorods enabled true correlation with the topographical information obtained by atomic force microscopy (AFM). All nanorods were analyzed in-situ on the same substrate using the same experimental parameters which allowed for accurate comparison. ZnO:Ga nanorods displayed the largest SE emission intensity as well as the greatest BSE emission intensity. Hydrogen plasma treatment reduced both SE and BSE emission intensity, whereas oxygen plasma treatment only reduced SE emission. These effects may help elucidate various optical as well as biological interactions of ZnO:Ga nanorods.
Klíčová slova:
correlative microscopy; SEM; AFM; ZnO nanorods; plasma treatment
Plné texty jsou dostupné na jednotlivých ústavech Akademie věd ČR.
Correlative probe electron microscopy analysis of plasma-treated gallium-doped zinc oxide nanorods
Correlative Probe Electron Microscopy (CPEM) was used to investigate the topographical and electronic emission properties of gallium-doped zinc oxide nanorods (ZnO:Ga) after low pressure hydrogen or ...
Application of In situ TR Spectroelectrochemical Techniques in Determination of Redox Mechanism of Bioactive Compounds
Sokolová, Romana; Jiroušková, Eliška; Degano, I.; Wantulok, J.; Nycz, J.
2023 - anglický
The electron transfer reactions play an important role in many natural processes. Reactions such as \ndissociation, protonation, and reactions with water and other small molecules often occur in \nbiotransformation. The reaction schemes involving these chemical reactions coupled to the \nelectron transfer can be determined by cyclic voltammetry. Additionally, in \nsitu spectroelectrochemistry can efficiently contribute to the determination of oxidation or \nreduction mechanism. This technique provides information about the electroactive chromophore during \nthe redox process allowing to identification the first reaction intermediates. The final reaction \nproducts were identified by chromatographic techniques. This study represents a key role of TR \nspectroelectrochemistry in the determination of reaction intermediates in the case of \n1,10- phenanthroline derivative substituted by bioactive phenothiazine unit and \ndrug 3- fluorophenmetrazine (2-(3-fluorophenyl)-3-methylmorpholine, 3-FPM). Co pound 3-FPM\nhave recently appeared as the new psychoactive substance in the drug market.\n
Klíčová slova:
IR spectroelectrochemistry; psychoactive substances; oxidation mechanism
Plné texty jsou dostupné na vyžádání prostřednictvím repozitáře Akademie věd.
Application of In situ TR Spectroelectrochemical Techniques in Determination of Redox Mechanism of Bioactive Compounds
The electron transfer reactions play an important role in many natural processes. Reactions such as \ndissociation, protonation, and reactions with water and other small molecules often occur in ...
A polarizable reference electrode
Mareček, Vladimír
2023 - anglický
New concept of a reference electrode for electrochemical systems resolves a problem of a poor \npotential stability of refence electrodes based on the distribution of a strongly \nhydrophobic common cation between two immiscible electrolyte solutions (TTTES). The use of a \npolarizable metal electrode instead of a classical reference electrode is demonstrated in \n a modified conventional four-electrode cell with TTTES. A simple battery operated potentiostat \ncontrols the working electrode potential in a three-electrode configuration. The working metal \nelectrode then serves as a polarizable reference organic solvent electrode in a four-electrode \nsystem for the polarization of the water/organic solvent interface.\n\n
Klíčová slova:
reference electrode; liquid/liquid interface; chloride extraction
Plné texty jsou dostupné na vyžádání prostřednictvím repozitáře Akademie věd.
A polarizable reference electrode
New concept of a reference electrode for electrochemical systems resolves a problem of a poor \npotential stability of refence electrodes based on the distribution of a strongly ...
Determination of Selected Natural Psychoactive Substances in Organic Matrices at 3D Printed Electrodes
Choińska-Mlynarczyk, Marta; Šestáková, Ivana; Navrátil, Tomáš
2023 - anglický
Psilocybin and its derivative psilocin are popular psychoactive substances both as experimental\ntreatments in clinical trials and as illicit drugs. Their potential ability to influence the human\nbrain entails the need for a fast, inexpensive, selective, and sensitive method of their\ndetermination. The aim of our study was the development of new 3D-printed electrodes which\nfulfill these demands and are useful for medical, toxicological, and forensic purposes.\nSuccessful development allows determining in real matrices (human plasma and dried\nmushrooms) concentrations of the order of 1 μmol dm-3.\n
Klíčová slova:
natural psychoactive substances; 3D-printed electrodes; psilocin; psilocybin
Plné texty jsou dostupné na vyžádání prostřednictvím repozitáře Akademie věd.
Determination of Selected Natural Psychoactive Substances in Organic Matrices at 3D Printed Electrodes
Psilocybin and its derivative psilocin are popular psychoactive substances both as experimental\ntreatments in clinical trials and as illicit drugs. Their potential ability to influence the ...
Ceramic protection of anti-corrosion layers of 3-glycidyloxypropyl-triethoxysilane on steel
Pokorný, P.; Prodanović, N.; Janata, Marek; Brožek, Vlastimil
2023 - anglický
There are various variations on the problem of steel reinforcement bond strength in concrete. Along with geometrical considerations, corrosion performance of steels with varying chemical compositions in interaction with variable chemical compositions of concrete are crucial. One approach is to cover steel surfaces with organosilane compounds, which increases the reinforcement resistance to corrosion in both acidic and alkaline conditions but, on the other hand, may weaken the reinforcement bond strength on concrete. The issue is resolved by intentionally forming a thin-walled, highly adhering corundum layer that is highly porous and impregnated with 3-glycidyloxypropyltriethoxysilane. This procedure also includes testing the adhesion properties between the ceramic and the metal and the cement prior to conducting a corrosion test in a chloride environment.
Klíčová slova:
steel; concrete; ceramics
Plné texty jsou dostupné na jednotlivých ústavech Akademie věd ČR.
Ceramic protection of anti-corrosion layers of 3-glycidyloxypropyl-triethoxysilane on steel
There are various variations on the problem of steel reinforcement bond strength in concrete. Along with geometrical considerations, corrosion performance of steels with varying chemical compositions ...
Measurements on KR-D-11B Optimized Subsonic Blade Cascade
Šimurda, David; Hála, Jindřich
2023 - anglický
This report contains results and evaluation of aerodynamic measurements conducted on a subsonic compressor blade cascade.
Klíčová slova:
compressor blade cascade; experiment; subsonic flow; optimized profile
Plné texty jsou dostupné na jednotlivých ústavech Akademie věd ČR.
Measurements on KR-D-11B Optimized Subsonic Blade Cascade
This report contains results and evaluation of aerodynamic measurements conducted on a subsonic compressor blade cascade.
Infants' learning of novel segments is modulated by prosody
Chládková, Kateřina; Podlipský, V.J.; Nudga, Natalia; Paillereau, Nikola; Kynčlová, Kateřina; Šimáčková, Š.
2023 - anglický
Young infants recognize atypical realisations of native-language speech. Later they learn words better from native-accented talkers. However, 6-month-olds preferentially listen to unfamiliar speech. We tested whether the learning of new vowels matches 6-month-olds’ listening preferences, being more effective from nonnative-accented speech. We exposed Czech six-month-olds to delexicalised utterances with consonants replaced by [f] and vowels by 405 tokens sampled from a bimodal [ɛ]-[æ] distribution, a contrast absent from Czech, and with either native or atypical rhythm. Discrimination of [ɛ]-[æ] was then tested in an alternating/non-alternating paradigm. Longer first-look duration to non-alternating than to alternating trials – indicating a learning effect – was found in infants familiarised with the novel contrast in atypical rhythm, such effect was not\ndetected after familiarisation with native rhythm. Six-month-olds thus more effectively exploit distributional information about novel vowels from non-native rhythm, which matches their previously reported preferences for listening to novel over familiar accents.
Klíčová slova:
distributional learning; selective learning; non-native rhythm; vowels; infancy
Plné texty jsou dostupné na vyžádání prostřednictvím repozitáře Akademie věd.
Infants' learning of novel segments is modulated by prosody
Young infants recognize atypical realisations of native-language speech. Later they learn words better from native-accented talkers. However, 6-month-olds preferentially listen to unfamiliar speech. ...
2TDK Railway, profile P18. Datings. Final Report.
Bosák, Pavel; Zupan Hajna, N.; Hercman, H.; Horáček, I.; Kdýr, Šimon; Kogovšek, B.
2023 - anglický
Samples for datings were taken in the railway construction (2TDK) near village of Divača, Classical Karst on October 12, 2021: (1) vertebrate bones in cave 2TDK – 002 at the profile P18, cave entrance appeared during the construction operations on cleaned karst surface in a wall of karst depression. Samples of mammal bones and gastropods were collected in situ on cave bottom, and (2) pieces of speleothems occurring in non in situ position on artificially planated surface near the cave opening were collected. U-series: no numerical date was obtained as geochemistry of sample indicate open system, probably due to recrystallization of sample in soil cover. Paleomagnetism: The transition of N- and R-polarized samples cannot be identified more precisely as U-series radiometric dating yielded no numerical results. The transition easily can represent Brunhes/Matuyama boundary (at 773 ka) as well as any of older such transitions (e. g., base of Jaramillo, base of Olduvai). In any case the speleothem grew in a closed cave space with roof, probably as flowstone (inclusion of red soils above the base) and later as baldachin on eroded allogenic fill of the paleocave. Vertebrate paleontology: bone remains of small and larger vertebrates represent subrecent to Holocene species. Sorex alpinus represents the species quite rare in fossil record, but recetly limited to variegated woodland habitats with high surface humidity. A chamois Rupicapra rupicapra represents a resident species present in Slovenia throughout all stages of a glacial cycle, recently restricted to mountain habitats.
Klíčová slova:
Divača Karst; unroofed cave; speleothem; U-Th dating; paleomagnetism; zoopaleontology
Plné texty jsou dostupné na jednotlivých ústavech Akademie věd ČR.
2TDK Railway, profile P18. Datings. Final Report.
Samples for datings were taken in the railway construction (2TDK) near village of Divača, Classical Karst on October 12, 2021: (1) vertebrate bones in cave 2TDK – 002 at the profile P18, cave entrance ...
Room temperature ethanol detection using carbon materials
Kočí, Michal
2023 - anglický
Allotropic forms of carbon, in particular graphene oxide (GO) or nanocrystalline diamond (NCD), attracted the attention of many research groups due to their unique electronic structures and extraordinary physical and chemical properties, preferable for many different applications, including sensor devices. This work focuses on responses of various sensing layers (NCD with hydrogen termination (H-NCD), graphene oxide (GO), reduced graphene oxide (rGO), thiol-functionalized graphene oxide (GO-SH) and their hybrid structures to ethanol vapor with concentrations up to 100 ppm in synthetic air at room temperature. The measured parameters of the tested sensors, especially stability, reproducibility and regeneration, are compared and critically evaluated. The high sensitivity of tested sensors achieved at room temperature makes them very promising for monitoring ethanol vapor as well as other volatile substances (e.g., isopropyl-alcohol or acetone).
Klíčová slova:
gas sensor; nanocrystalline diamond (NCD); graphene oxide (GO); reduced graphene oxide (rGO); thiol-functionalized graphene oxide (GO-SH)
Plné texty jsou dostupné na jednotlivých ústavech Akademie věd ČR.
Room temperature ethanol detection using carbon materials
Allotropic forms of carbon, in particular graphene oxide (GO) or nanocrystalline diamond (NCD), attracted the attention of many research groups due to their unique electronic structures and ...
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